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OilLab 600 - Pensky Martens

ASTM D93 procedures A, B, C - ASTM D3941 - ASTM E502
DIN EN 22719
EN 22719
IP 34
ISO 2719
ISO 15267
JIS K 2265-3

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Subject

Flash Point on petroleum products, gas oils, fuel oils, lubrificants, biodiesel. Suitable for flash point detection on different substances, waste materials, solvents…

Measuring Pensky Martens Principle

The sample is heated and stirred at specified rates, using one of three defined procedures (A, B, or C). An ignition source is directed into the test cup at regular intervals with simultaneous interruption of the stirring, until a flash is detected.

Measuring Parameters

• Temperatures: in °C.
• Measuring range: ambient … +370°C.
• Resolution: 0.01 °C.
• Accuracy: ± 0.1 °C.
• Repeatability / Reproducibility: as per standards methods or bette.r

Ignition system

• Instrument equipped with flame ignition device made in brass, with 0.7 mm diameter orifice for analysis with gas also provided with electrical ignitor hot-wire that automatically passes through the center of large opening (A) of the proper cup cover.

Pilot Flame

• Secondary pilot flame gas propelled for re-enlight the test flame, alternatively elictrical ignitor hot wire shall be used; a bead of 4 mm is provided to compare flame dimensions.

Measuring Temperature Devices

• Sample temperature is measured with a platinum resistance PT100 Class A with SS sheath and high temperature resistant silicone cable.
• Bath temperature is measured with a PT100 sensor.

Dual flash point detection system

• By ionisation ring.
• By thermal sensor.

Barometric correction

• Barometric built-in sensor with automatic correction of results to a barometric pressure of 101.3 kPa automatically performed by the software at the end of analysis.

Heating

• Electrical heater with heating rates as per procedures A, B, C.

Cooling

• Built-in forced air fan at the end of the test.

Test Cup

• Made of brass with Ni-Cr treatment for more corrosion resistance and provided with an high temperature resistant handle.
• Internal diameter: 50.8 mm.
• External diameter: 54 mm.
• Internal depht: 55.8 mm.
• Filling mark at 21.8 mm from upper side.

Stirrer

• An electric motor drives a flexible transmission coil allowing the stirring of the product through a two-bladed metal propellers. Stirring speed as per selected procedures A, B, C.

Shutter

• Automatic mechanism opening the shutter for the dip-in of the ignition device.

Safety features

• Gas valve for closing the gas supply (max 30 mBar), at the end of the test.
• Overheating protection with auto shut off during the test.
• Auto fire detection by means of thermal fuse with acoustic alarm.

Software Features

• All analytical parameters recorded.
• Customizable analysis parameters and methods.
• Customizable results report.
• Printable graphs and results.

The software includes:

Analysis Menu

• Automatic execution of the analysis in accordance to the selected procedure (Standard method as per ASTM / IP / ISO / EN / DIN… norms of reference as well as costumized procedures).
• Automatic handling of samples with unknown flash point.
• Display in real time of all the analysis parameters and status.
• Fields for introduction of operator and product name.
• Expected flash point temperature programmable.
• Audible alarm and displayed messages at the end of the analysis and in case of errors and/or malfunctions.
• Configuration menu with up to 20 preset samples and expected flash point.
• Automatic barometric correction of results.

Diagnostic Menu

• Direct access to all analog, digital, inputs and outputs.
• Selectable value displaying: °C / Volt.

Calibration Menu

• Automatic calibration of each temperature probe.
• Up to 100 calibration points (standard with 5 and dynamic with up to 100 points).
• Programmable calibration frequency with selectable validity period and notice/lock-down at expiration date.
• Last calibration date referred to each single probe displayed and relevant data printable.
• Display of calibration diagram.

Data utilities

• Archive viewer for files recall.
• All analysis stored in Excel® compatible format as well as in jpg format.
• LIMS compatible.

Integrated Touch Screen Panel PC

• TFT/LCD 8"
• Resolution 1024 × 768, 16.2 M colours
• 2 × USB port for connection to an external printer and/or external PC + 1 Ethernet RJ45
• Storage capacity for more than 60’000 analysis.

Electrical Supply

• 220 V or 115 V ± 15% / 50 to 60 Hz.
• Cord cable with schuko plug.

Ambient Temperature

• Max 35°C.
• H.R. 80%.

Dimensions

• width 30 cm.
• depth 48 cm.
• height 52 cm.

Weight

• 27 kg.

Accessories for Line Connection

• 5050: Gas reducer 30 mbar.
• 5052: Gas connection tube, 5 m.

Tools Required for Routine Calibration

• 3013: Calibration decade box - PT100 simulator.
• 3102: Kit of connectors and cables.
• 3096: Digital thermometer reader with LCD display for PT100, PT1000, Resolution 0.01°C, accuracy 0.01°C, read up to +650°C – single channel.
• 3779: PT100 sensor for immersion, temperature range -196…+500°C, 3 mm diameter, 300 mm length.
• 5273: Digital tachometer, Contact and Non-Contact.
  • Digital 5-digit 13 mm LCD display with backlight.
  • Non-contact rotation speed (RPM), total revolutions (REV), Frequency (Hz), Surface speed (m/min, ln/min, Ft/min, Yd/min) and length (m, In, Ft, Yd).
  • 40 reading memories: Max, Min, Avg, Data.
  • Detecting distance: 50…500 mm.
  • Speed range: up to 99 with 0.001 scale, up to 999 with 0.01 scale, up to 9999 with 0,1 scale, up to 199’999 with 1 scale (value in rpm/min).
  • Accuracy: +/- 0.05% +/- 1 digit.
  • Dimensions: 6.0 × 16.0 × 4.0 cm.
  • Weight 160 g.
  • Power: battery 9 V.

Reference Sample

• 7715: Certified reference material Pensky-Martens Closed Cup, ASTM D93 procedure A; Product Nature: Mineral Oil; Pack size: 3 × 80 ml; Certified value: +80.0 °C approx.
• 7562: Certified reference material Pensky-Martens Closed Cup, ASTM D93 procedure A; Product nature: Mineral Oil; Pack size: 3 × 80 ml; Certified Value: +105.0 °C approx.
• 7563: Certified reference material Pensky-Martens Closed Cup, ASTM D93 procedure A; Product nature: Mineral oil; Pack size: 3 × 80 ml; Certified value: +140.0 °C approx.
• 7716: Certified reference material Pensky-Martens Closed Cup, ASTM D93 procedure A; Product nature: Mineral Oil; Pack Size: 3 × 80 ml; Certified value: +230.0 °C approx.

Spare Parts

• 7172: Electrical ignitor for PM long life.
• 5319: Test cup made in treated brass with internal level mark and handle.
• 7170: Flexible stirrer with connection joints.
• 7175: PT100 sensor, A Class, made in stainless steel with connector.
• 7369: Detection - ionisation cable.
• 3158: Heater collar 420 W, 220 Vac.
• 3157: Heater collar 420 W, 115 Vac.
• 3150: PT100 temperature sensor for bath temperature.
• 3047: Motor for stirrer.
• 3171: Fan Element 220 vac.
• 3173: Fan Element 110 vac.
• 5321: Complete cover with movement.
• 3754: Thermal detector.
• 17028: Security thermal fuses.
• 5031+3051: Gas valve with solenoid (220 Vac).
• 5031+3155: Gas valve with solenoid (110 Vac).
• 15979: Gas ignitor.
• 3836: PCB Fuses, box of 10 pcs.
• 7671: Silicone tubing, 1 m.
• 16881: Support PT 100 Teflon.
• 7750: OilLab adhesive protection for screen sticked.

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